(R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

Base Information

Chemical Name:(R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide
CAS No.:923601-68-7
Molecular Formula:C₁₇H₂₅NO₄S
Molecular Weight:339.456
Hs Code.:

Synonyms:(R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

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Chemical Property of (R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

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Technology Process of (R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

There total 7 articles about (R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 3674-18-8
Boc-D-pheO-succinyl

: 5034-06-0
trimethyl sulfoxonium chloride

: 923601-68-7
(R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

Guidance literature:: trimethyl sulfoxonium chloride; With potassium tert-butylate; In tetrahydrofuran; at 90 ℃; for 2h;

Boc-D-pheO-succinyl; In tetrahydrofuran; at -20 ℃;

Reference yield:

: 1774-47-6
trimethylsulfoxonium iodide

: 16159-70-9
N-tert-butoxycarbonyl D-phenylalanine p-nitrophenyl ester

: 923601-68-7
(R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

Guidance literature:: trimethylsulfoxonium iodide; With potassium tert-butylate; In tetrahydrofuran; for 3h; Heating / reflux;

N-tert-butoxycarbonyl D-phenylalanine p-nitrophenyl ester; In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

: 1247065-58-2
C₁₈H₂₈NO₇P

: 1774-47-6
trimethylsulfoxonium iodide

: 923601-68-7
(R)-dimethylsulfoxonium 2-oxo-3-(tert-butoxycarbonylamino)-4-phenylbutylide

: 400611-25-8
tert-butyl (S)-(4-(dimethyl(oxo)-λ6-sulfanylidene)-3-oxo-1-phenylbutan-2-yl)carbamate

Guidance literature:: trimethylsulfoxonium iodide; With potassium tert-butylate; In tetrahydrofuran; at 90 ℃; for 2h;

C₁₈H₂₈NO₇P; In tetrahydrofuran; at -20 ℃;