11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

Base Information

Chemical Name:11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one
CAS No.:906374-89-8
Molecular Formula:C₂₈H₃₄O₇
Molecular Weight:482.574
Hs Code.:

Synonyms:11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

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Chemical Property of 11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

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Technology Process of 11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

There total 4 articles about 11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 936913-81-4
4-(tert-butyl-diphenyl-silanyloxy)-2-chloromethyl-6-hydroxy-benzoic acid 1-methyl-but-3-enyl ester

: 906374-89-8
11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / TBAF / tetrahydrofuran / 0.5 h / 23 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1002/anie.200600593

Reference yield:

: 64584-92-5
(R)-pent-4-en-2-ol

: 906374-89-8
11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / DIAD; 2-furylphosphine / benzene / 12 h

2: 100 percent / TBAF / tetrahydrofuran / 0.5 h / 23 °C

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; (2-furyl)phosphine; In tetrahydrofuran; benzene; 1: Mitsunobu esterification;
DOI:10.1002/anie.200600593

Reference yield:

: 378749-93-0
4-tert-butyldiphenylsiloxy-2-chloromethyl-6-hydroxybenzoic acid

: 906374-89-8
11-benzyloxy-2-ethoxymethoxy-4,12-dihydroxy-7-methyl-7,8,11,12,13,14-hexahydro-6-oxa-benzocyclotetradecen-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / DIAD; 2-furylphosphine / benzene / 12 h

2: 100 percent / TBAF / tetrahydrofuran / 0.5 h / 23 °C

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; (2-furyl)phosphine; In tetrahydrofuran; benzene; 1: Mitsunobu esterification;
DOI:10.1002/anie.200600593