1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

Base Information

Chemical Name:1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine
CAS No.:315238-80-3
Molecular Formula:C₃₆H₆₀B₂N₂O₂
Molecular Weight:574.507
Hs Code.:

Synonyms:1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

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Technology Process of 1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

There total 3 articles about 1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 315238-61-0
(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

: 315238-80-3
1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

Guidance literature:: With tert-butyl lithium; In hexane; byproducts: LiCl, t-C4H9H; tert-BuLi was added dropwise to a soln. of amino(halo)(oraganyloxy)borane in hexane at -78°C, the mixt. was allowed to warm to room temp., stirring was continued under 0°C (N2); sublimed, elem. anal.;
DOI:10.1021/om0005912

Reference yield:

: 128-39-2
2,6-di-tert-butylphenol

: 315238-80-3
1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

Guidance literature:: Multi-step reaction with 3 steps

1: ethyldiisopropylamine / diethyl ether

2: n-butyl lithium / hexane

3: tert-butyl lithium / hexane

With ethyldiisopropylamine; n-butyl lithium; tert-butyl lithium; In diethyl ether; hexane;
DOI:10.1021/om0005912

Reference yield:

: 315238-73-4
(tert-butylamino)(2,6-di-tert-butylphenyloxy)(fluoro)borane

: 315238-80-3
1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

Guidance literature:: With tert-butyl lithium; In hexane; byproducts: LiF, t-C4H9H; tert-BuLi was added dropwise to a soln. of amino(halo)(oraganyloxy)borane in hexane at -78°C, the mixt. was allowed to warm to room temp., stirring was continued under 0°C, 24 h (N2); crystals were washed with hexane; elem. anal.;
DOI:10.1021/om0005912