(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

Base Information

Chemical Name:(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane
CAS No.:315238-61-0
Molecular Formula:C₁₈H₃₁BClNO
Molecular Weight:323.714
Hs Code.:

Synonyms:(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

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Chemical Property of (tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

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Technology Process of (tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

There total 1 articles about (tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 24415-36-9
2,6-(t-C₄H₉)2C₆H₃OBCl₂

: 75-64-9
tert-butylamine

: 315238-61-0
(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

Guidance literature:: With n-butyl lithium; In hexane; byproducts: LiCl; an equimolar amounts of n-BuLi was added to a soln. amine in hexane, refluxed for 3 h, cooled to -78°C, a soln. of dihalogeno-oxyboranein hexane was added dropwise, stirred for 2 h then allowed to warm (N2); the solvent was removed at reduced pressure, distd. twice; elem. anal.;
DOI:10.1021/om0005912

Reference yield: 63.0%

: 315238-61-0
(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

: 4648-54-8
trimethylsilylazide

: 315238-94-9
azido(2,6-di-tert-butylphenoxy)[tert-butyl(trimethylsilyl)amino]borane

Guidance literature:: With tert-butyl lithium; In hexane; byproducts: LiCl, tert-butane; a soln. of aminoborane in hexane was cooled to -78°C, (CH3)3SiN3was added, then tert-butyllithium, the mixt. was allowed to warm to room temp. with stirring (N2); the solvent was removed, the residue was sublimed in vac. (90°C/0.01 Torr); elem. anal.;
DOI:10.1021/om0005912

Reference yield: 62.0%

: 315238-61-0
(tert-butylamino)(2,6-tert-butylphenyloxy)(chloro)borane

: 315238-80-3
1,3-di-tert-butyl-2,4-bis(2,6-di-tert-butylphenoxy)-1,3-diaza-2,4-diboretidine

Guidance literature:: With tert-butyl lithium; In hexane; byproducts: LiCl, t-C4H9H; tert-BuLi was added dropwise to a soln. of amino(halo)(oraganyloxy)borane in hexane at -78°C, the mixt. was allowed to warm to room temp., stirring was continued under 0°C (N2); sublimed, elem. anal.;
DOI:10.1021/om0005912