allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

Base Information

Chemical Name:allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside
CAS No.:705932-36-1
Molecular Formula:C₂₅H₃₀FNO₅
Molecular Weight:443.515
Hs Code.:

Synonyms:allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

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Chemical Property of allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

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Technology Process of allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

There total 7 articles about allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 705932-48-5
allyl 2-acetamido-2-deoxy-3,6-di-O-benzyl-4-mesyl-α-D-glucopyranoside

: 705932-36-1
allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; for 60h; Heating;
DOI:10.1039/b402860k

Reference yield:

: 63064-50-6
allyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 705932-36-1
allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaBH₃CN; 4 Angstroem molecular sieves / tetrahydrofuran / 0.33 h / 20 °C

1.2: 69 percent / aq. HCl / tetrahydrofuran; diethyl ether / 1 h / 20 °C / pH 3

2.1: 92 percent / pyridine / 4.17 h / -13 - 0 °C

3.1: 71 percent / tetrabutylammonium fluoride / acetonitrile / 60 h / Heating

With pyridine; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium cyanoborohydride; In tetrahydrofuran; acetonitrile;
DOI:10.1039/b402860k

Reference yield:

: 63064-49-3
allyl 2-acetamido-2-deoxy-4,6-O-benzylidene-α-D-glucopyranoside

: 705932-36-1
allyl 2-acetamido-2,4-dideoxy-3,6-di-O-benzyl-4-fluoro-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: 76 percent / BaO; Ba(OH)2 / dimethylformamide / 12 h / 20 °C

2.1: NaBH₃CN; 4 Angstroem molecular sieves / tetrahydrofuran / 0.33 h / 20 °C

2.2: 69 percent / aq. HCl / tetrahydrofuran; diethyl ether / 1 h / 20 °C / pH 3

3.1: 92 percent / pyridine / 4.17 h / -13 - 0 °C

4.1: 71 percent / tetrabutylammonium fluoride / acetonitrile / 60 h / Heating

With pyridine; barium dihydroxide; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium cyanoborohydride; barium(II) oxide; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b402860k