(E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

Base Information

Chemical Name:(E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)
CAS No.:1402424-07-0
Molecular Formula:C₂₈H₃₄N₂O₄S₂
Molecular Weight:526.721
Hs Code.:

Synonyms:(E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

Suppliers and Price of (E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

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Technology Process of (E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

There total 1 articles about (E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 821-06-7
(E)-1,4-dibromobutene

: 321707-21-5
2,4,6-trimethyl-N-(prop-2-yn-1-yl)benzenesulfonamide

: 1402424-07-0
(E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201201031

Reference yield:

: 1402424-07-0
(E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

: C₂₈H₃₄N₂O₄S₂

Guidance literature:: With BF₄^(1-)*C₂₂H₃₆NO₂PRhS⁽¹⁺⁾; trifluoroacetic acid; In dichloromethane; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Reflux;
DOI:10.1002/anie.201201031

Reference yield:

: 1402424-07-0
(E)-N,N'-(but-2-ene-1,4-diyl)bis(4-methyl-N-(prop-2-yn-1-yl)benzenesulfonamide)

: C₂₈H₃₄N₂O₄S₂

: C₂₈H₃₄N₂O₄S₂

Guidance literature:: With tetrafluoroboric acid; BF₄^(1-)*C₂₂H₃₆NO₂PRhS⁽¹⁺⁾; In dichloromethane; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Reflux;
DOI:10.1002/anie.201201031