methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

Base Information

Chemical Name:methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate
CAS No.:1091599-62-0
Molecular Formula:C₁₆H₁₅Cl₂NO₃
Molecular Weight:340.206
Hs Code.:

Synonyms:methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

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Chemical Property of methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

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Technology Process of methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

There total 8 articles about methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22109-55-3
3,5-dichloro-6-methyl-1H-pyridin-2-one

: 1065269-88-6
methyl 4-(2-iodoethyl)benzoate

: 1091599-62-0
methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

Guidance literature:: 3,5-dichloro-6-methyl-1H-pyridin-2-one; With sodium hydride; lithium bromide; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h;

methyl 4-(2-iodoethyl)benzoate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; mineral oil; at 20 - 65 ℃;

Reference yield:

: 1091599-89-1
methyl 4-[2-(6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

: 1091599-62-0
methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

Guidance literature:: With N-chloro-succinimide; acetic acid; In water; at 20 - 70 ℃;

Reference yield:

: 675-10-5
4-hydroxy-6-methyl-2-pyron

: 1091599-62-0
methyl 4-[2-(3,5-dichloro-6-methyl-2-oxopyridin-1(2H)-yl)ethyl]benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water / 0.25 h / 20 °C

1.2: 24 h / 80 °C

1.3: 0.5 h

2.1: sulfuric acid / 4 h / Heating; Reflux

3.1: pyridine / 3 h / 5 °C

4.1: hydrogen; N-ethyl-N,N-diisopropylamine / palladium 10% on activated carbon / ethyl acetate; water

5.1: N-chloro-succinimide; acetic acid / water / 20 - 70 °C

With pyridine; N-chloro-succinimide; sulfuric acid; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; palladium 10% on activated carbon; In water; ethyl acetate;