C₃₇H₂₈N₆O₄

Base Information

Chemical Name:C₃₇H₂₈N₆O₄
CAS No.:112089-50-6
Molecular Formula:C₃₇H₂₈N₆O₄
Molecular Weight:620.667
Hs Code.:

C<sub>37</sub>H<sub>28</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₃₇H₂₈N₆O₄

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Chemical Property of C₃₇H₂₈N₆O₄

Chemical Property:

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Technology Process of C₃₇H₂₈N₆O₄

There total 20 articles about C₃₇H₂₈N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4993-93-5
4-nitro-1H-indole-2-carboxylic acid ethyl ester

: 112089-50-6
C₃₇H₂₈N₆O₄

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / hydrogen / PtO₂ / ethanol; tetrahydrofuran / 3.25 h / 724.01 Torr

2: 81 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / dimethylformamide / 48 h

3: 97 percent / aq. KOH / methanol; dimethylformamide / 0.5 h

4: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / dimethylformamide / 48 h

5: 51 percent / aq. KOH / dimethylformamide

6: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride

7: (dimethylamino)pyridine / pyridine

8: 1.) trimethylsilyl chloride, NaI, 2.) triethylamine / 1.) acetonitrile, reflux, 30 min, 2.) 30 min

With dmap; potassium hydroxide; chloro-trimethyl-silane; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide; platinum(IV) oxide; In tetrahydrofuran; pyridine; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00398a017

Reference yield:

: 610-78-6
3-nitro-4-chlorophenol

: 112089-50-6
C₃₇H₂₈N₆O₄

Guidance literature:: Multi-step reaction with 14 steps

1: 96 percent / K₂CO₃ / acetone; dimethylformamide / 64 h / Ambient temperature

2: 77 percent / NaH / dimethylsulfoxide / 24 h / 105 - 115 °C

3: 40 percent / diisobutylaluminum hydride / tetrahydrofuran / 2.3 h / Ambient temperature

4: 69 percent / hydrogen / 84.5percent PtO₂ / ethanol / 2.75 h / 2327.2 Torr

5: 111 g / pyridine / 1.42 h / 5 °C

6: 1.) sodium acetate, 2.) triethylamine / 1.) ethanol, reflux, 20 h, 2.) methylene chloride

7: 64 percent / nitric acid / nitromethane / 0.67 h / 0 °C

8: 81 percent / hydrogen / 84.5percent PtO₂ / tetrahydrofuran; ethanol / 2 h / 2068.6 Torr

9: 1.) sulfuryl chloride, 2.) 1,8-bis(dimethylamino)naphthalene / 1.) methylene chloride, -70 deg C, 45 min, 2.) -70 deg C, 4 h

10: 90 percent / borane-methyl sulfide, 4-Angstroem molecular sieves / tetrahydrofuran / 3 h / Heating

11: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran; toluene

12: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride

13: (dimethylamino)pyridine / pyridine

14: 1.) trimethylsilyl chloride, NaI, 2.) triethylamine / 1.) acetonitrile, reflux, 30 min, 2.) 30 min

With pyridine; dmap; chloro-trimethyl-silane; sulfuryl dichloride; dimethylsulfide borane complex; 4 A molecular sieve; hydrogen; nitric acid; sodium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide; platinum(IV) oxide; In tetrahydrofuran; pyridine; nitromethane; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/jm00398a017

Reference yield:

: 106014-83-9
2-[4-(benzyloxy)-2-nitrophenyl]propane-1,3-diol

: 112089-50-6
C₃₇H₂₈N₆O₄

Guidance literature:: Multi-step reaction with 11 steps

1: 69 percent / hydrogen / 84.5percent PtO₂ / ethanol / 2.75 h / 2327.2 Torr

2: 111 g / pyridine / 1.42 h / 5 °C

3: 1.) sodium acetate, 2.) triethylamine / 1.) ethanol, reflux, 20 h, 2.) methylene chloride

4: 64 percent / nitric acid / nitromethane / 0.67 h / 0 °C

5: 81 percent / hydrogen / 84.5percent PtO₂ / tetrahydrofuran; ethanol / 2 h / 2068.6 Torr

6: 1.) sulfuryl chloride, 2.) 1,8-bis(dimethylamino)naphthalene / 1.) methylene chloride, -70 deg C, 45 min, 2.) -70 deg C, 4 h

7: 90 percent / borane-methyl sulfide, 4-Angstroem molecular sieves / tetrahydrofuran / 3 h / Heating

8: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran; toluene

9: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride

10: (dimethylamino)pyridine / pyridine

11: 1.) trimethylsilyl chloride, NaI, 2.) triethylamine / 1.) acetonitrile, reflux, 30 min, 2.) 30 min

With pyridine; dmap; chloro-trimethyl-silane; sulfuryl dichloride; dimethylsulfide borane complex; 4 A molecular sieve; hydrogen; nitric acid; sodium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide; platinum(IV) oxide; In tetrahydrofuran; pyridine; nitromethane; ethanol; toluene;
DOI:10.1021/jm00398a017