tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt

Base Information

• Chemical Name: tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt
• CAS No.: 852312-78-8
• Molecular Formula: C₃₆H₃₂BN₂₀*Na
• Molecular Weight: 778.585
• Mol file: 852312-78-8.mol

Synonyms:tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt

Chemical Property of tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt

There total 4 articles about tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

potassium tetrakis(4-cyanophenyl)borate + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) → tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt (852312-78-8)

Guidance literature:

potassium tetrakis(4-cyanophenyl)borate; N-Cyanoguanidine; With potassium hydroxide; In 2-methoxy-ethanol; for 18h; Heating;

With sodium chloride;

DOI:10.1021/ja042233m

Reference yield: 87.0%

potassium tetrakis(4-cyanophenyl)borate + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) + sodium chloride (7647-14-5) → tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt (852312-78-8)

Guidance literature:

With KOH; In further solvent(s); mixt. of potassium tetrakis(4-cyanophenyl)borate, dicyandiamide and KOH in 2-methoxyethanol refluxed under N2 for 18 h; solvent evapd. under reduced pressure; ppt. washed with MeOH, dried and redissolved in boiling water and satd. aq. NaCl added; suspn. filtered, solid washed with water and dried in vac.; recrystd. from water;

DOI:10.1021/ja042233m

Reference yield:

lithium tetrakis(4-iodophenyl)borate → tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate sodium salt (852312-78-8)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / palladium diacetate / further solvent(s)

2: KOH / further solvent(s)

With KOH; palladium diacetate; In further solvent(s);

DOI:10.1021/ja042233m

upstream raw materials:

N-Cyanoguanidine

sodium chloride

para-diiodobenzene

Downstream raw materials:

potassium tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate

lithium tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate

phenazinium tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate

N(CH₃(CH₂)3)⁽¹⁺⁾ tetrakis[4-[2-(4,6-diamino-1,3,5-triazinyl)]phenyl]borate