phenyltitanate

Base Information

Chemical Name:phenyltitanate
CAS No.:2371-72-4
Molecular Formula:C₂₄H₂₀Ti
Molecular Weight:356.303
Hs Code.:

Synonyms:phenyltitanate

Suppliers and Price of phenyltitanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyltitanate

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Technology Process of phenyltitanate

There total 3 articles about phenyltitanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 7550-45-0
titanium tetrachloride

: 555-54-4
diphenylmagnesium

: 2371-72-4
phenyltitanate

Guidance literature:: In 1,4-dioxane; diethyl ether; toluene; under Ar, addn. of toluene to ether soln. of Ph2Mg; cooled to -40°C, dropwise addn. of toluene soln. of TiCl4 with stirring (1h), addn. of some dioxane, further stirred 30 min; left overnight at -78°C, filtered at -40°C in cooled evacuated ampoule, left 1d at -78°C, crystn., filtn., washing (pentane), drying in vac. at -20°C;