[(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]

Base Information

Chemical Name:[(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]
CAS No.:288155-73-7
Molecular Formula:C₂₉H₂₉OP₂Pd*C₃₂H₁₂BF₂₄
Molecular Weight:1425.14
Hs Code.:

[(1,3-bis(diphenylphosphino)propane)Pd(CH<sub>3</sub>)(CO)][B(3,5-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4]

Synonyms:[(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]

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Chemical Property of [(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]

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Technology Process of [(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]

There total 2 articles about [(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex

: 113530-46-4
cis-dimethylbis(PPh₂C₃H₆PPh₂)palladium(II)

: 201230-82-2
carbon monoxide

: 288155-73-7
[(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: In dichloromethane; under Ar, the Pd intermediate was produced in situ by the react. of dimethyl complex and HB((CF3)2C6H3)4*2O(C2H5)2 at -30°C, the soln. was cooled to -90°C, CO was added for 5 min; the soln. was purged with Ar for 30 min, hexane was added to ppt. the product; elem. anal.;
DOI:10.1021/ja994251n

Reference yield:

: 260993-77-9
[(1,3-bis(diphenylphosphino)propane)palladium(methyl)((CH₃CH₂)2O)][B(3,5-(CF₃)2C₆H₃)4]

: 201230-82-2
carbon monoxide

: 288155-73-7
[(1,3-bis(diphenylphosphino)propane)Pd(CH₃)(CO)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: In dichloromethane; under Ar; a soln. of Pd complex in CH2Cl2 was purged with CO at -90°C; excess CO was removed by purging the soln. with Ar at -90°C;
DOI:10.1021/om010489k