1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

Base Information

Chemical Name:1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine
CAS No.:76453-34-4
Molecular Formula:C₂₀H₂₈N₂O₆
Molecular Weight:392.452
Hs Code.:

Synonyms:1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

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Chemical Property of 1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

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Technology Process of 1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

There total 8 articles about 1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 76453-40-2
4-(1-Ethoxy-ethoxymethyl)-3-(6-methoxycarbonyl-hexyl)-2-oxo-imidazolidine-1-carboxylic acid benzyl ester

: 76453-34-4
1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 1h; Ambient temperature;

Reference yield: 73.0%

: 76453-33-3
methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

: 76453-34-4
1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1.5h;

Reference yield:

: 54049-24-0
methyl 7-bromoheptanoate

: 76453-34-4
1-benzyloxycarbonyl-4-hydroxymethyl-3-(6-methoxycarbonyl)hexyl-2-oxoimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / 65percent NaH, KI / dimethylformamide / 48 h / 60 °C

2: 73 percent / NaBH₄ / ethanol / 1.5 h / 0 °C

With sodium tetrahydroborate; sodium hydride; potassium iodide; In ethanol; N,N-dimethyl-formamide;