methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

Base Information

Chemical Name:methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate
CAS No.:76453-33-3
Molecular Formula:C₂₁H₂₈N₂O₇
Molecular Weight:420.463
Hs Code.:

Synonyms:methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

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Chemical Property of methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

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Technology Process of methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

There total 4 articles about methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 54049-24-0
methyl 7-bromoheptanoate

: 76453-28-6
methyl 1-benzyloxycarbonyl-2-oxo-4-imidazolidinecarboxylate

: 76453-33-3
methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

Guidance literature:: With sodium hydride; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 48h;

Reference yield: 46.0%

: 54049-24-0
methyl 7-bromoheptanoate

: 76453-27-5
methyl 3-benzyloxycarbonyl-2-oxo-4-imidazolidinecarboxylate

: 76453-33-3
methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

Guidance literature:: With sodium hydride; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 48h;

Reference yield:

: 76497-31-9
2-oxo-imidazolidine-1,5-dicarboxylic acid 1-benzyl ester

: 76453-33-3
methyl 1-benzyloxycarbonyl-3-(6-methoxycarbonyl)hexyl-2-oxo-4-imidazolidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / SOCl₂ / 1.) 4 h, room temp., 2.) 3 h, reflux

2: 46 percent / 65percent NaH, KI / dimethylformamide / 48 h / 60 °C

With thionyl chloride; sodium hydride; potassium iodide; In N,N-dimethyl-formamide;