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N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone

Base Information Edit
  • Chemical Name:N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone
  • CAS No.:90105-46-7
  • Molecular Formula:C14H17 N3 O3
  • Molecular Weight:275.307
  • Hs Code.:
  • Mol file:90105-46-7.mol
N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone

Synonyms:Carbamicacid, [(1S)-3-diazo-1-(1-methylethyl)-2-oxopropyl]-, phenylmethyl ester (9CI);Carbamic acid, [3-diazo-1-(1-methylethyl)-2-oxopropyl]-, phenylmethyl ester,(S)-

Suppliers and Price of N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
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  • price
Total 5 raw suppliers
Chemical Property of N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone Edit
Chemical Property:
  • PSA:92.79000 
  • LogP:2.27906 
Purity/Quality:

98% *data from raw suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone

There total 6 articles about N-alpha-Benzyloxycarbonyl-L-valinyl-diazomethane, (3S)-3-Z-amino-1-diazo-4-methyl-2-pentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
(S)-N-(benzyloxycarbonyl)valine; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; diethyl ether; at -25 ℃; for 0.5h;
diazomethane; In tetrahydrofuran; diethyl ether; at -10 - 20 ℃; for 3h;
DOI:10.1016/j.tetasy.2005.01.049
Guidance literature:
Multi-step reaction with 2 steps
1: Et3N / diethyl ether; tetrahydrofuran / 0.5 h / -25 °C
2: diethyl ether / 3 h / -10 °C
With triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.3390/12051183
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