diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

Base Information

Chemical Name:diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate
CAS No.:134361-29-8
Molecular Formula:C₃₀H₃₉O₈PS
Molecular Weight:590.675
Hs Code.:

diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-<diphenyl(4-methoxyphenyl)methoxy>butyl>phosphonate

Synonyms:diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

Chemical Property:

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Technology Process of diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

There total 5 articles about diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 134361-28-7
diethyl <4-hydroxy-3-butyl>phosphonateyl

: 124-63-0
methanesulfonyl chloride

: 134361-29-8
diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

Guidance literature:: With TEA; In dichloromethane; 1.) -20 deg C, 30 min, 2.) 25 deg C, 1 h;
DOI:10.1021/jm00111a052

Reference yield:

: 97845-58-4
5-(2-bromoethyl)-2,2-dimethyl-1,3-dioxane

: 134361-29-8
diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium iodide / acetone / 16 h / 25 °C

2: 0.67 h / 140 °C

3: 2 N HCl / acetone / 1 h / 25 °C

4: 30 percent / pyridine, TEA, 4-(dimethylamino)pyridine / 2 h / 60 °C

5: 93 percent / TEA / CH₂Cl₂ / 1.) -20 deg C, 30 min, 2.) 25 deg C, 1 h

With pyridine; hydrogenchloride; dmap; TEA; sodium iodide; In dichloromethane; acetone;
DOI:10.1021/jm00111a052

Reference yield:

: 2-(2,2-dimethyl-1,3-dioxan-5-yl)ethyl iodide

: 134361-29-8
diethyl <3-<<(methanesulfonyl)oxy>methyl>-3-butyl>phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: 0.67 h / 140 °C

2: 2 N HCl / acetone / 1 h / 25 °C

3: 30 percent / pyridine, TEA, 4-(dimethylamino)pyridine / 2 h / 60 °C

4: 93 percent / TEA / CH₂Cl₂ / 1.) -20 deg C, 30 min, 2.) 25 deg C, 1 h

With pyridine; hydrogenchloride; dmap; TEA; In dichloromethane; acetone;
DOI:10.1021/jm00111a052