4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

Base Information

Chemical Name:4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester
CAS No.:226396-44-7
Molecular Formula:C₂₃H₂₇NO₇S
Molecular Weight:461.536
Hs Code.:

4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-<i>tert</i>-butyl ester

Synonyms:4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

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Chemical Property of 4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

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Technology Process of 4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

There total 4 articles about 4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 226396-42-5
1-tert-butyl 4-ethyl 4-[(4-phenoxyphenyl)sulfonyl]piperidine-1,4-dicarboxylate

: 226396-44-7
4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; ethanol; at 65 ℃; for 16h;
DOI:10.1021/jm0500875

Reference yield:

: 226396-40-3
1-tert-butyl 4-ethyl 4-[(4-phenoxyphenyl)thio]piperidine-1,4-dicarboxylate

: 226396-44-7
4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: 100 percent / aq. NaOH / ethanol; tetrahydrofuran / 16 h / 65 °C

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm0500875

Reference yield:

: 113113-66-9
1,2-bis(4-phenoxyphenyl)disulfane

: 226396-44-7
4-(4-phenoxy-benzenesulfonyl)-piperidine-1,4-dicarboxylic acid mono-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 2 h / -45 - 0 °C

1.2: 86 percent / tetrahydrofuran / 17 h / 0 - 20 °C

2.1: 87 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / 0 - 20 °C

3.1: 100 percent / aq. NaOH / ethanol; tetrahydrofuran / 16 h / 65 °C

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm0500875