4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

Base Information

Chemical Name:4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine
CAS No.:950772-33-5
Molecular Formula:C₂₁H₃₅N₃O
Molecular Weight:345.528
Hs Code.:

4-ethyl-N<sub>2</sub>-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

Synonyms:4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

Suppliers and Price of 4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

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Technology Process of 4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

There total 4 articles about 4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 950772-32-4
N-(5-ethenyl-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

: 950772-33-5
4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

Guidance literature:: N-(5-ethenyl-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine; With ammonium formate; In methanol; at 20 ℃; for 0.166667h;

palladium 10% on activated carbon; In methanol; for 0.5h;

Reference yield:

: 321-23-3
4-bromo-2-fluoronitrobenzene

: 950772-33-5
4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 80 °C

2.1: triphenylphosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 20 - 120 °C

3.1: ammonium formate / methanol / 0.17 h / 20 °C

3.2: 0.5 h

With ammonium formate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 950772-30-2
N-(5-bromo-2-nitrophenyl)-1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinamine

: 950772-33-5
4-ethyl-N₂-{1-[trans-4-(ethyloxy)cyclohexyl]-4-piperidinyl}-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 20 - 120 °C

2.1: ammonium formate / methanol / 0.17 h / 20 °C

2.2: 0.5 h

With ammonium formate; triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In methanol; toluene;