Technology Process of 1,3-diphenyl-6-(9H-2-fluoren-yl)fulvene
There total 3 articles about 1,3-diphenyl-6-(9H-2-fluoren-yl)fulvene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyrrolidine;
In
ethanol;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jo301101x
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
1.2: 0.08 h
2.1: pyrrolidine / ethanol / 20 °C / Inert atmosphere
With
pyrrolidine;
In
tetrahydrofuran; ethanol;
DOI:10.1021/jo301101x
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium cyanide / N,N-dimethyl-formamide / 0.33 h / 35 °C / Inert atmosphere
1.2: 4.33 h / 35 °C / Inert atmosphere
2.1: sodium hydroxide / water / 4 h / Reflux
3.1: tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
3.2: 0.08 h
4.1: pyrrolidine / ethanol / 20 °C / Inert atmosphere
With
pyrrolidine; sodium cyanide; sodium hydroxide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
1.1: Stetter coupling / 1.2: Stetter coupling;
DOI:10.1021/jo301101x
