1,3-Benzenediamine, N1,N3-diethyl-2-nitro-

Base Information

• Chemical Name: 1,3-Benzenediamine, N1,N3-diethyl-2-nitro-
• CAS No.: 908590-74-9
• Molecular Formula: C10H15 N3 O2
• Molecular Weight: 0
• Mol file: 908590-74-9.mol

Synonyms:1,3-Benzenediamine,N,N'-diethyl-2-nitro- (9CI); N,N'-Diethyl-2-nitrobenzene-1,3-diamine

Chemical Property of 1,3-Benzenediamine, N1,N3-diethyl-2-nitro-

Chemical Property:

• PSA: 69.88000
• LogP: 3.12760

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Benzenediamine, N1,N3-diethyl-2-nitro-

There total 2 articles about 1,3-Benzenediamine, N1,N3-diethyl-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2,6-difluoro-1-nitrobenzene (19064-24-5) + ethylamine (75-04-7,85404-22-4) → N,N'-diethyl-2-nitrobenzene-1,3-diamine (908590-74-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl acetamide; toluene; at 119.84 ℃; for 3h;

DOI:10.1107/S0108270108008275

Reference yield:

2,6-difluoroaniline (5509-65-9) + ethylamine (75-04-7,85404-22-4) → N-ethyl-3-fluoro-2-nitroaniline (929565-74-2) + N,N'-diethyl-2-nitrobenzene-1,3-diamine (908590-74-9)

Guidance literature:

In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃;

upstream raw materials:

2,6-difluoroaniline

ethylamine

2,6-difluoro-1-nitrobenzene

Refernces

• 1、 Walczak, Christopher P.,Yonkey, Matthew M.,Squattrito, Philip J.,Mohanty, Dillip K.,Kirschbaum, Kristin. "1,3-Bis(ethyl-amino)-2-nitro-benzene, 1,3-bis-(n-octylamino)-2-nitro- benzene and 4-ethylamino-2-methyl-1H-benz-imid-azole". . p. o248-o251. Retrieved 2008/09/21.