C₅₀H₆₃N₄O₁₅PSSi

Base Information

Chemical Name:C₅₀H₆₃N₄O₁₅PSSi
CAS No.:1054662-32-6
Molecular Formula:C₅₀H₆₃N₄O₁₅PSSi
Molecular Weight:1051.19
Hs Code.:

C<sub>50</sub>H<sub>63</sub>N<sub>4</sub>O<sub>15</sub>PSSi

Synonyms:C₅₀H₆₃N₄O₁₅PSSi

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Chemical Property of C₅₀H₆₃N₄O₁₅PSSi

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Technology Process of C₅₀H₆₃N₄O₁₅PSSi

There total 14 articles about C₅₀H₆₃N₄O₁₅PSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40733-27-5
3'-O-(t-butyldimethylsilyl)thymidine

: 541541-19-9
1-[(5R,7R,9S)-11-Diisopropylamino-2,2-bis-(4-methoxy-phenyl)-15,15-dioxo-3,6,10,12-tetraoxa-15λ⁶-thia-11-phospha-tricyclo[15.3.1.0^5,9]henicosa-1(20),17(21),18-trien-7-yl]-5-methyl-1H-pyrimidine-2,4-dione

: 1054662-32-6
C₅₀H₆₃N₄O₁₅PSSi

Guidance literature:: With 1H-tetrazole; In acetonitrile; at 20 ℃; for 0.0833333h;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1054662-32-6
C₅₀H₆₃N₄O₁₅PSSi

Guidance literature:: Multi-step reaction with 13 steps

1.1: magnesium / tetrahydrofuran / 1 h / 20 °C

1.2: 81 percent / tetrahydrofuran / 1 h / 0 - 20 °C

2.1: acetyl chloride / 1 h / Heating

3.1: 43.2 g / pyridine / 0 °C

4.1: 77 percent Spectr_. / N-bromosuccinimide; N,N'-azobisisobutyronitrile / CCl₄ / 0.33 h / Heating

5.1: 21.5 g / N-ethyldiisopropylamine / dimethylformamide / 3 h / 20 °C

6.1: 82 percent / m-chloroperbenzoic acid; sodium bicarbonate / CH₂Cl₂ / 0.25 h / 0 °C

7.1: 97 percent / imidazole / dimethylformamide / 1 h / 20 °C

8.1: 88 percent / trifluoroacetic acid / CH₂Cl₂ / 0.17 h / 20 °C

9.1: acetyl chloride / toluene / 1 h / Heating

10.1: 1.06 g / pyridine / 3 h / 20 °C

11.1: 94 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C

12.1: 45 percent / molecular sieves 4 Angstroem; N-ethyldiisopropylamine / CH₂Cl₂ / 2 h / Heating

13.1: 1H-tetrazole / acetonitrile / 0.08 h / 20 °C

With pyridine; 1H-imidazole; 1H-tetrazole; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; magnesium; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 99-36-5
1-methoxycarbonyl-3-methylbenzene

: 1054662-32-6
C₅₀H₆₃N₄O₁₅PSSi

Guidance literature:: Multi-step reaction with 13 steps

1.1: magnesium / tetrahydrofuran / 1 h / 20 °C

1.2: 81 percent / tetrahydrofuran / 1 h / 0 - 20 °C

2.1: acetyl chloride / 1 h / Heating

3.1: 43.2 g / pyridine / 0 °C

4.1: 77 percent Spectr_. / N-bromosuccinimide; N,N'-azobisisobutyronitrile / CCl₄ / 0.33 h / Heating

5.1: 21.5 g / N-ethyldiisopropylamine / dimethylformamide / 3 h / 20 °C

6.1: 82 percent / m-chloroperbenzoic acid; sodium bicarbonate / CH₂Cl₂ / 0.25 h / 0 °C

7.1: 97 percent / imidazole / dimethylformamide / 1 h / 20 °C

8.1: 88 percent / trifluoroacetic acid / CH₂Cl₂ / 0.17 h / 20 °C

9.1: acetyl chloride / toluene / 1 h / Heating

10.1: 1.06 g / pyridine / 3 h / 20 °C

11.1: 94 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C

12.1: 45 percent / molecular sieves 4 Angstroem; N-ethyldiisopropylamine / CH₂Cl₂ / 2 h / Heating

13.1: 1H-tetrazole / acetonitrile / 0.08 h / 20 °C

With pyridine; 1H-imidazole; 1H-tetrazole; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; magnesium; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;