6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

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Chemical Name:6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione
CAS No.:1613132-92-5
Molecular Formula:C₂₀H₁₈N₆O₂S
Molecular Weight:406.468
Hs Code.:

Synonyms:6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

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Chemical Property of 6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

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Technology Process of 6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

There total 6 articles about 6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1613132-86-7
C₁₇H₁₄N₆O₂S

: 106-95-6
allyl bromide

: 1613132-92-5
6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

Guidance literature:: With zinc; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.ejmech.2014.04.043

Reference yield:

: 4993-87-7
5-nitro-2-phenyl-1H-indole

: 1613132-92-5
6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / toluene / Reflux

2: sodium hydroxide / ethanol / 8 h / Reflux

3: potassium permanganate; ammonia / 0.25 h / 0 °C

4: zinc / tetrahydrofuran / 20 °C

With potassium permanganate; ammonia; potassium carbonate; sodium hydroxide; zinc; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/j.ejmech.2014.04.043

Reference yield:

: 1613132-74-3
C₁₆H₁₁ClN₂O₃

: 1613132-92-5
6-(3-allyl-5-nitro-2-phenyl-1H-indol-1-yl)-5-amino-4,5-dihydro-1,2,4-triazine-3(2H)-thione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 8 h / Reflux

2: potassium permanganate; ammonia / 0.25 h / 0 °C

3: zinc / tetrahydrofuran / 20 °C

With potassium permanganate; ammonia; sodium hydroxide; zinc; In tetrahydrofuran; ethanol;
DOI:10.1016/j.ejmech.2014.04.043