N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

Base Information

Chemical Name:N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)
CAS No.:1582301-41-4
Molecular Formula:C₂₃H₃₂N₂O₂Si
Molecular Weight:396.605
Hs Code.:

Synonyms:N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

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Chemical Property of N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

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Technology Process of N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

There total 1 articles about N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1346686-33-6
N,N'-(4,6-bis((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

: 1346686-34-7
N,N'-(4,6-diethynyl-1,3-phenylene)bis(2,2-dimethylpropanamide)

: 1582301-41-4
N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja500125r

Reference yield:

: 1044811-15-5
1-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-3,5-diazidobenzene

: 1582301-41-4
N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

: C₅₉H₈₂N₁₀O₈Si₂

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; water; tert-butyl alcohol; at 60 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ja500125r

Reference yield:

: 1582301-41-4
N,N'-(4-ethynyl-6-((trimethylsilyl)ethynyl)-1,3-phenylene)bis(2,2-dimethylpropanamide)

: 1582301-42-5
C₅₃H₆₆N₁₀O₈

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / tert-butyl alcohol; tetrahydrofuran; water / 2.5 h / 60 °C / Inert atmosphere

2: potassium carbonate / methanol; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1021/ja500125r