2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Base Information

Chemical Name:2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate
CAS No.:103434-73-7
Molecular Formula:C₂₀H₂₀N₄O₉
Molecular Weight:460.4
Hs Code.:

Synonyms:2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

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Chemical Property of 2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

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Technology Process of 2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

There total 4 articles about 2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.7%

: 193539-61-6
(Z)-3-Amino-but-2-enoic acid 2-cyano-ethyl ester

: 147597-18-0
2-nitrooxyethyl-2-(3-nitrobenzylidene)acetoacetate

: 103434-73-7
2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: In isopropyl alcohol; for 3h; Heating;
DOI:10.1248/cpb.41.108

Reference yield:

: 88488-47-5
2-bromoethyl acetoacetate

: 103434-73-7
2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 87.4 percent / AgNO₃ / acetonitrile / 48 h / Ambient temperature

2: AcOH, piperidine / benzene / 2 h / Heating

3: 69.7 percent / propan-2-ol / 3 h / Heating

With piperidine; silver nitrate; acetic acid; In isopropyl alcohol; acetonitrile; benzene;
DOI:10.1248/cpb.41.108

Reference yield:

: 88488-48-6
2-nitrooxyethyl 3-oxobutanoate

: 103434-73-7
2-nitrooxyethyl 2-cyanoethyl 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH, piperidine / benzene / 2 h / Heating

2: 69.7 percent / propan-2-ol / 3 h / Heating

With piperidine; acetic acid; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.41.108