5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Base Information

Chemical Name:5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside
CAS No.:299409-68-0
Molecular Formula:C₂₀H₂₇NO₆
Molecular Weight:377.437
Hs Code.:

Synonyms:5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

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Chemical Property of 5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

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Technology Process of 5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

There total 2 articles about 5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 299409-46-4
N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

: 299409-68-0
5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Guidance literature:: With pyridine; at 20 ℃; for 2h;
DOI:10.1080/00397910008087449

Reference yield:

: 162920-12-9,191997-35-0
(Z)-N-(5-deoxy-2,3-0-isopropylidene-l-O-methyl-D-yxo-l,4-furanose-5-ylidene)benzylamine N-oxide

: 299409-68-0
5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Et₂AlCl / diethyl ether / 2 h / -30 °C

2: 100 percent / pyridine / 2 h / 20 °C

With pyridine; diethylaluminium chloride; In diethyl ether; 1: Addition / 2: Acetylation;
DOI:10.1080/00397910008087449

Reference yield:

: 299409-68-0
5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

: 1053709-95-7
C₁₉H₂₅NO₈

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; at 0 ℃; for 0.5h;
DOI:10.1080/00397910008087449