N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Base Information

• Chemical Name: N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside
• CAS No.: 299409-46-4
• Molecular Formula: C₁₈H₂₅NO₅
• Molecular Weight: 335.4

Synonyms:N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Chemical Property of N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

There total 1 articles about N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

vinyl magnesium bromide (1826-67-1) + (Z)-N-(5-deoxy-2,3-0-isopropylidene-l-O-methyl-D-yxo-l,4-furanose-5-ylidene)benzylamine N-oxide (162920-12-9,191997-35-0) → N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-β-L-gulo-1,4-pentofuranoside + N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside (299409-46-4)

Guidance literature:

With diethylaluminium chloride; In diethyl ether; at -30 ℃; for 2h;

DOI:10.1080/00397910008087449

Reference yield: 100.0%

acetic anhydride (108-24-7) + N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside (299409-46-4) → 5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside (299409-68-0)

Guidance literature:

With pyridine; at 20 ℃; for 2h;

DOI:10.1080/00397910008087449

Reference yield: 80.0%

N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside (299409-46-4) → 5-benzylamino-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Guidance literature:

With copper diacetate; zinc; In acetic acid; at 70 ℃; for 1h;

DOI:10.1080/00397910008087449

upstream raw materials:

vinyl magnesium bromide

(Z)-N-(5-deoxy-2,3-0-isopropylidene-l-O-methyl-D-yxo-l,4-furanose-5-ylidene)benzylamine N-oxide

Downstream raw materials:

5-(acetoxyamino)-N-benzyl-5-deoxy-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 299409-46-4 N-benzyl-5-deoxy-5-(hydroxylamino)-5-vinyl-2,3-O-isopropylidene-1-O-methyl-α-D-manno-1,4-pentofuranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send