[4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

Base Information

Chemical Name:[4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine
CAS No.:902143-21-9
Molecular Formula:C₃₂H₄₂BrNO₂Si
Molecular Weight:580.68
Hs Code.:

Synonyms:[4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

Suppliers and Price of [4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of [4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

There total 4 articles about [4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 866475-57-2
[2-bromomethyl-3-(4-bromophenyl)propoxy]-tert-butyldimethylsilane

: 33365-53-6
(E)-4-(4-(dimethylamino)styryl)phenol

: 902143-21-9
[4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1021/jm050166g

Reference yield:

: 866475-55-0
2-(4-bromobenzyl)propane-1,3-diol

: 902143-21-9
[4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 370 mg / Et₃N / CH₂Cl₂ / 20 °C

2: CBr₄; PPh₃; pyridine / CH₂Cl₂ / 20 °C

3: K₂CO₃ / dimethylformamide / 100 °C

With pyridine; carbon tetrabromide; potassium carbonate; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050166g

Reference yield:

: 866475-56-1
3-(4-bromophenyl)-2-(tert-butyldimethylsilanyloxymethyl)propan-1-ol

: 902143-21-9
[4-(2-{4-[2-(4-bromobenzyl)-3-(tert-butyldimethylsilanyloxy)propoxy]phenyl}vinyl)phenyl]dimethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: CBr₄; PPh₃; pyridine / CH₂Cl₂ / 20 °C

2: K₂CO₃ / dimethylformamide / 100 °C

With pyridine; carbon tetrabromide; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050166g