3-(acetyloxy)-4-nitrobenzyl [(tert-butoxycarbonyl)amino]acetate

Base Information

Chemical Name:3-(acetyloxy)-4-nitrobenzyl [(tert-butoxycarbonyl)amino]acetate
CAS No.:182913-44-6
Molecular Formula:C₁₆H₂₀N₂O₈
Molecular Weight:368.343
Hs Code.:
Mol file:182913-44-6.mol

Synonyms:1-acetoxy-5-(tert-butoxycarbonylaminoacetoxymethyl)-2-nitrobenzene

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Chemical Property of 3-(acetyloxy)-4-nitrobenzyl [(tert-butoxycarbonyl)amino]acetate

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Technology Process of 3-(acetyloxy)-4-nitrobenzyl [(tert-butoxycarbonyl)amino]acetate

There total 2 articles about 3-(acetyloxy)-4-nitrobenzyl [(tert-butoxycarbonyl)amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 700-38-9
2-nitro-5-methylphenol

: 182913-44-6
1-acetoxy-5-(tert-butoxycarbonylaminoacetoxymethyl)-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine / Heating; 1-1.5 h

2: 1.) N-bromosuccinimide, azobis(isobutyronitrile), 2.) K₂CO₃, tetrabutylammonium bromide / 1.) methyl acetate, reflux, 2.) DMF, 18-20 deg C, 1-1.5 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; potassium carbonate; triethylamine;

Reference yield:

: 4530-20-5
BOC-glycine

: 182913-38-8
5-methyl-2-nitrophenyl acetate

: 1-acetoxy-5-dibromomethyl-2-nitrobenzene

: 182913-44-6
1-acetoxy-5-(tert-butoxycarbonylaminoacetoxymethyl)-2-nitrobenzene

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); tetrabutylammomium bromide; potassium carbonate; Yield given. Multistep reaction; 1.) methyl acetate, reflux, 2.) DMF, 18-20 deg C, 1-1.5 h;