(S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate

Base Information

• Chemical Name: (S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate
• CAS No.: 1414969-69-9
• Molecular Formula: C₂₃H₂₆N₄O₄S
• Molecular Weight: 454.55
• Mol file: 1414969-69-9.mol

Synonyms:(S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate

Chemical Property of (S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate

There total 1 articles about (S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + 2-amino-N-(benzo[d]thiazol-2-yl)acetamide hydrochloride (1228794-16-8) → (S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate (1414969-69-9)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2012.09.035

Reference yield: 90.0%

(S)-tert-butyl (1-((2-(benzo[d]thiazol-2-ylamino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate (1414969-69-9) → C18H18N4O2S*ClH (1414969-71-3)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 4h;

DOI:10.1016/j.bmc.2012.09.035

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

2-amino-N-(benzo[d]thiazol-2-yl)acetamide hydrochloride

Downstream raw materials:

C₁₈H₁₈N₄O₂S*ClH