(9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

Base Information

Chemical Name:(9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate
CAS No.:881921-05-7
Molecular Formula:C₃₂H₄₃NO₂
Molecular Weight:473.699
Hs Code.:

Synonyms:(9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

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Chemical Property of (9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

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Technology Process of (9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

There total 6 articles about (9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 881921-02-4
(1S,2S,4R)-2-((S,E)-3-isocyanato-3-methylhex-1-enyl)-1-isopropyl-4-methylcyclohexane

: 24324-17-2
9-Fluorenylmethanol

: 881921-05-7
(9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

Guidance literature:: With titanium(IV) tetrabutoxide; In benzene; at 45 ℃; for 3h;
DOI:10.1021/ol053061g

Reference yield:

: 881920-66-7
(S,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-2-en-1-ol

: 881921-05-7
(9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / N-methylmorpholine N-oxide; tetrapropylammonium perruthenate; molecular sieves 4 Angstroem / CH₂Cl₂ / 0.58 h / 20 °C

2: 21 mg / lithium triethylborohydride / tetrahydrofuran / 0.33 h / -78 °C

3: CH₂Cl₂ / 1 h / 0 °C

4: 426 mg / potassium carbonate / methanol; H₂O / 0 - 23 °C

5: 99 percent / trifluoroacetic anhydride; triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

6: 84 percent / titanium(IV) tert-butoxide / benzene / 3 h / 45 °C

With titanium(IV) tetrabutoxide; tetrapropylammonium perruthennate; 4 A molecular sieve; lithium triethylborohydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1021/ol053061g

Reference yield:

: 881920-68-9
(R,E)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-2-en-1-ol

: 881921-05-7
(9H-fluoren-9-yl)methyl (S,E)-1-((1S,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methylhex-1-en-3-ylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: CH₂Cl₂ / 1 h / 0 °C

2: 426 mg / potassium carbonate / methanol; H₂O / 0 - 23 °C

3: 99 percent / trifluoroacetic anhydride; triethylamine / CH₂Cl₂ / 0.25 h / 0 °C

4: 84 percent / titanium(IV) tert-butoxide / benzene / 3 h / 45 °C

With titanium(IV) tetrabutoxide; potassium carbonate; triethylamine; trifluoroacetic anhydride; In methanol; dichloromethane; water; benzene;
DOI:10.1021/ol053061g