1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone

Base Information

Chemical Name:1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone
CAS No.:1297599-15-5
Molecular Formula:C₂₂H₉ClF₆O₈S₂
Molecular Weight:614.884
Hs Code.:

Synonyms:1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone

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Chemical Property of 1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone

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Technology Process of 1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone

There total 2 articles about 1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1297598-99-2
1,2,4-tris[(trifluoromethylsulfonyl)oxy]anthraquinone

: 63503-60-6
3-chlorophenylboronic acid

: 1297599-15-5
1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 95 ℃; for 10h; regioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201001497

Reference yield:

: 81-54-9
1,2,4-trihydroxy-9,10-anthraquinone

: 1297599-15-5
1,2-bis[(trifluoromethylsulfonyl)oxy]-4-(3-chlorophenyl)anthraquinone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere

2: potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 10 h / 95 °C / Inert atmosphere

With pyridine; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; dichloromethane; 2: Suzuki-Miyaura coupling;
DOI:10.1002/ejoc.201001497