C₂₃H₂₃F₄N₃O₇S₂

Base Information

Chemical Name:C₂₃H₂₃F₄N₃O₇S₂
CAS No.:1374233-65-4
Molecular Formula:C₂₃H₂₃F₄N₃O₇S₂
Molecular Weight:593.577
Hs Code.:

C<sub>23</sub>H<sub>23</sub>F<sub>4</sub>N<sub>3</sub>O<sub>7</sub>S<sub>2</sub>

Synonyms:C₂₃H₂₃F₄N₃O₇S₂

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Chemical Property of C₂₃H₂₃F₄N₃O₇S₂

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Technology Process of C₂₃H₂₃F₄N₃O₇S₂

There total 7 articles about C₂₃H₂₃F₄N₃O₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1374233-64-3
C₂₂H₂₄FN₃O₅S

: 1374233-65-4
C₂₃H₂₃F₄N₃O₇S₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; dmap; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 31872-62-5
4-methoxy-3-nitro-pyridine

: 1374233-65-4
C₂₃H₂₃F₄N₃O₇S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 24 h / 20 °C

2.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

3.1: dichloromethane / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

6.1: 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Reflux

6.2: 0 °C / pH 3 - 4

7.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 0.5 h / 0 °C

With 2-(diethylamino)ethanethiol hydrochloride; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; dmap; palladium 10% on activated carbon; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 33631-09-3
4-methoxypyridin-3-amine

: 1374233-65-4
C₂₃H₂₃F₄N₃O₇S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2.1: dichloromethane / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

5.1: 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere; Reflux

5.2: 0 °C / pH 3 - 4

6.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 0.5 h / 0 °C

With 2-(diethylamino)ethanethiol hydrochloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; dmap; In dichloromethane; N,N-dimethyl-formamide;