2-(trifluoromethyl)phenylselenyl cyanate

Base Information

Chemical Name:2-(trifluoromethyl)phenylselenyl cyanate
CAS No.:215655-72-4
Molecular Formula:C₈H₄F₃NSe
Molecular Weight:250.082
Hs Code.:

Synonyms:2-(trifluoromethyl)phenylselenyl cyanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(trifluoromethyl)phenylselenyl cyanate

Chemical Property:

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Technology Process of 2-(trifluoromethyl)phenylselenyl cyanate

There total 3 articles about 2-(trifluoromethyl)phenylselenyl cyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3425-46-5
potassium selenocyanate

: 88-17-5
2-(trifluoromethyl)benzenamine

: 215655-72-4
2-(trifluoromethyl)phenylselenyl cyanate

Guidance literature:: 2-(trifluoromethyl)benzenamine; With hydrogenchloride; sodium nitrite; at 0 ℃; for 1h;

potassium selenocyanate; With sodium acetate; pH=6; Further stages.;
DOI:10.1021/ja016348r

Reference yield:

: o-(trifluoromethyl)benzenediazonium tetrafluoroborate

: 3425-46-5
potassium selenocyanate

: 215655-72-4
2-(trifluoromethyl)phenylselenyl cyanate

Guidance literature:: With 1,10-Phenanthroline; caesium carbonate; copper(l) chloride; copper dichloride; In acetonitrile; at -25 - 20 ℃; for 0.5h; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201504601

Reference yield:

: 88-17-5
2-(trifluoromethyl)benzenamine

: 215655-72-4
2-(trifluoromethyl)phenylselenyl cyanate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrafluoroboric acid diethyl ether; isopentyl nitrite / ethanol / 0.25 h / -15 - 0 °C

2: caesium carbonate; copper(l) chloride; copper dichloride; 1,10-Phenanthroline / acetonitrile / 0.5 h / -25 - 20 °C / Glovebox; Inert atmosphere; Sealed tube

With tetrafluoroboric acid diethyl ether; 1,10-Phenanthroline; caesium carbonate; copper(l) chloride; copper dichloride; isopentyl nitrite; In ethanol; acetonitrile;
DOI:10.1002/chem.201504601