2-(5-phenyl)furylmethyl propargyl ether

Base Information

Chemical Name:2-(5-phenyl)furylmethyl propargyl ether
CAS No.:533934-24-6
Molecular Formula:C₁₄H₁₂O₂
Molecular Weight:212.248
Hs Code.:

Synonyms:2-(5-phenyl)furylmethyl propargyl ether

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Chemical Property of 2-(5-phenyl)furylmethyl propargyl ether

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Technology Process of 2-(5-phenyl)furylmethyl propargyl ether

There total 5 articles about 2-(5-phenyl)furylmethyl propargyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 22078-90-6
2-hydroxymethyl-5-phenylfuran

: 106-96-7
propargyl bromide

: 533934-24-6
2-(5-phenyl)furylmethyl propargyl ether

Guidance literature:: 2-hydroxymethyl-5-phenylfuran; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

propargyl bromide; In N,N-dimethyl-formamide; toluene; at 23 ℃; for 16h;
DOI:10.1021/ja029125p

Reference yield:

: 1899-24-7
5-bromo-2-furancarboxaldehyde

: 533934-24-6
2-(5-phenyl)furylmethyl propargyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / benzyltrimethylammonium bromide; Pd(OAc)2; aq. K₂CO₃ / 3 h

2.1: 99 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

3.1: NaH / dimethylformamide / 0.5 h / 0 °C

3.2: 71 percent / dimethylformamide; toluene / 16 h / 23 °C

With palladium diacetate; lithium aluminium tetrahydride; trimethylbenzylammonium bromide; sodium hydride; potassium carbonate; In diethyl ether; N,N-dimethyl-formamide; 1.1: Suzuki coupling;
DOI:10.1021/ja029125p

Reference yield:

: 13803-39-9
5-phenylfuran-2-carbaldehyde

: 533934-24-6
2-(5-phenyl)furylmethyl propargyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 99 percent / LiAlH₄ / diethyl ether / 1 h / 0 °C

2.1: NaH / dimethylformamide / 0.5 h / 0 °C

2.2: 71 percent / dimethylformamide; toluene / 16 h / 23 °C

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja029125p