2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Base Information

Chemical Name:2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride
CAS No.:74615-81-9
Molecular Formula:C₁₉H₁₉ClN₆O₉
Molecular Weight:510.848
Hs Code.:

Synonyms:2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Suppliers and Price of 2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

There total 7 articles about 2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 102735-31-9
1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

: 74615-81-9
2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Guidance literature:: With hydrogenchloride; acetyl chloride; In diethyl ether; for 18h;
DOI:10.1246/bcsj.55.1156

Reference yield: 82.0%

: 74615-80-8
1-O-acetyl-2,6-bis-N-(2,4-dinitrophenyl)-6-epi-purpurosamine B

: 74615-81-9
2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Guidance literature:: With hydrogenchloride; acetyl chloride; In diethyl ether;
DOI:10.1246/cl.1980.641

Reference yield:

: 64307-85-3
methyl 2,6-bis(acetamido)-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

: 74615-81-9
2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranosyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / 1 M HCl / 15 h / Heating

2: boron trifluoride / diethyl ether / 12 h

3: triethylamine / methanol; H₂O / 16 h

4: 82 percent / HCl, acetyl chloride / diethyl ether / 18 h

With hydrogenchloride; boron trifluoride; triethylamine; acetyl chloride; In methanol; diethyl ether; water;
DOI:10.1246/bcsj.55.1156