1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

Base Information

Chemical Name:1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose
CAS No.:102735-31-9
Molecular Formula:C₂₁H₂₂N₆O₁₁
Molecular Weight:534.439
Hs Code.:

Synonyms:1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

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Chemical Property of 1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

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Technology Process of 1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

There total 3 articles about 1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64307-85-3
methyl 2,6-bis(acetamido)-2,3,4,6,7-pentadeoxy-β-L-lyxo-heptopyranoside

: 102735-31-9
1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / 1 M HCl / 15 h / Heating

2: boron trifluoride / diethyl ether / 12 h

3: triethylamine / methanol; H₂O / 16 h

With hydrogenchloride; boron trifluoride; triethylamine; In methanol; diethyl ether; water;
DOI:10.1246/bcsj.55.1156

Reference yield:

: 6-epi-D-purpurosamine B dihydrochloride

: 102735-31-9
1-O-acetyl-2,6-bis(2,4-dinitrophenylamino)-2,3,4,6,7-pentadeoxy-L-lyxo-heptapyranose

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride / diethyl ether / 12 h

2: triethylamine / methanol; H₂O / 16 h

With boron trifluoride; triethylamine; In methanol; diethyl ether; water;
DOI:10.1246/bcsj.55.1156