1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

Base Information

Chemical Name:1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone
CAS No.:1402404-47-0
Molecular Formula:C₂₀H₃₂O₂Si
Molecular Weight:332.558
Hs Code.:

Synonyms:1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

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Technology Process of 1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

There total 4 articles about 1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 617-86-7
triethylsilane

: 1402404-16-3
3-(3-(cyclohex-1-en-1-yl)prop-2-yn-1-ylidene)pentane-2,4-dione

: 1402404-47-0
1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

Guidance literature:: In toluene; at 140 ℃; for 4h; Microwave irradiation;
DOI:10.1002/adsc.201601037

Reference yield: 61.0%

: 617-86-7
triethylsilane

: 15341-64-7
3-(cyclohex-1-en-1-yl)propiolaldehyde

: 123-54-6,81235-32-7
acetylacetone

: 1402404-47-0
1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

Guidance literature:: With zinc(II) chloride; In neat (no solvent); at 60 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201501155

Reference yield:

: 15341-64-7
3-(cyclohex-1-en-1-yl)propiolaldehyde

: 1402404-47-0
1-(5-(cyclohex-1-en-1-yl(triethylsilyl)methyl)-2-methylfuran-3-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine; magnesium sulfate; acetic acid / toluene / 6 h / 30 °C / Inert atmosphere

2: zinc(II) chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

With piperidine; magnesium sulfate; acetic acid; zinc(II) chloride; In dichloromethane; toluene;
DOI:10.1002/anie.201203914