1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline
CAS No.:1283610-05-8
Molecular Formula:C₁₉H₂₃N
Molecular Weight:265.398
Hs Code.:

Synonyms:1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

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Chemical Property of 1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

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Technology Process of 1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

There total 2 articles about 1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 78-33-1
tri-p-tert-butylphenol phosphate ester

: 1283610-05-8
1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

Guidance literature:: With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; potassium carbonate; at 130 ℃; for 16h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.9b00703

Reference yield: 90.0%

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 1283610-05-8
1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

Guidance literature:: 1-bromo-4-tert-butylbenzene; With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In toluene; for 0.25h; Inert atmosphere; Heating;

1,2,3,4-tetrahydroisoquinoline; With sodium t-butanolate; In toluene; for 24h; Inert atmosphere; Heating;
DOI:10.1039/c0jm03109g

Reference yield: 92.0%

: 1283610-05-8
1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1283610-07-0
1-(4-tert-butylphenyl)-1,2,3,4-tetrahydroquinoline-6-carbaldehyde

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; for 0.5h; Inert atmosphere; Cooling with ice;

1-(4-(tert-butyl)phenyl)-1,2,3,4-tetrahydroquinoline; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c0jm03109g