S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide

Base Information

• Chemical Name: S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide
• CAS No.: 1147095-60-0
• Molecular Formula: C₂₁H₁₉ClN₄O₄S
• Molecular Weight: 458.925

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide

Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide

Chemical Property:

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide

There total 10 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-N-(5-chloro-pyridin-2-yl)-5-methoxy-benzamide (280773-17-3) → S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide (1147095-60-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

2: sulfuric acid / 0 - 5 °C

With sulfuric acid; In tetrahydrofuran;

DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

C29H25ClN4O6S → S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide (1147095-60-0)

Guidance literature:

With sulfuric acid; at 0 - 5 ℃;

DOI:10.1016/j.ejmech.2012.10.005

Reference yield:

methyl 4-(methylsulfinyl)benzoate (114129-35-0) → S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl sulfoximide (1147095-60-0)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

2: pyridine / dichloromethane; toluene / 3 h / 15 - 30 °C / Inert atmosphere

3: water; sodium hydroxide / tetrahydrofuran / 3 h / 25 - 30 °C

4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

5: tetrahydrofuran / 2 h / 10 - 30 °C / Inert atmosphere

6: sulfuric acid / 0 - 5 °C

With pyridine; sodium azide; oxalyl dichloride; sulfuric acid; water; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform; toluene;

DOI:10.1016/j.ejmech.2012.10.005

upstream raw materials:

methyl 4-(methylsulfinyl)benzoate

5-methoxy-2-nitro-benzoic acid

C₁₆H₁₄ClNO₄S

methyl 4-[imino(methyl)oxo-λ⁶-sulfanyl]benzoate

Downstream raw materials:

S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-methoxyphenyl}carbamoyl)phenyl]-S-methyl-N-(2-diethylamino-acetyl)sulfoximide

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