1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone

Base Information

• Chemical Name: 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone
• CAS No.: 1448165-00-1
• Molecular Formula: C₁₅H₁₄O₄S
• Molecular Weight: 290.34
• Mol file: 1448165-00-1.mol

Synonyms:1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone

Chemical Property of 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone

There total 11 articles about 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

o-methoxystyrene (612-15-7) + sodium benzenesulfonate (873-55-2) → 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone (1448165-00-1)

Guidance literature:

With dipotassium peroxodisulfate; water; at 20 ℃; for 18h;

DOI:10.1002/ejoc.201301833

Reference yield: 82.0%

o-methoxystyrene (612-15-7) + thiophenol (108-98-5) → 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone (1448165-00-1)

Guidance literature:

With dipotassium peroxodisulfate; oxygen; silver nitrate; In N,N-dimethyl-formamide; at 20 ℃; for 22h; Green chemistry;

DOI:10.1039/c4ob00776j

Reference yield: 81.0%

1-ethynyl-2-methoxybenzene (767-91-9) + sodium benzenesulfonate (873-55-2) → 1-(2-methoxyphenyl)-2-(phenylsulfonyl)-1-ethanone (1448165-00-1)

Guidance literature:

With iron(III) chloride; dipotassium peroxodisulfate; oxygen; In water; at 20 ℃; for 7h; Green chemistry;

DOI:10.1016/j.tetlet.2014.03.078

upstream raw materials:

1-ethynyl-2-methoxybenzene

Benzenesulfinic acid

o-methoxystyrene

sodium benzenesulfonate

Downstream raw materials:

1-(2-methoxyphenyl)prop-2-en-1-one