(1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

Base Information

Chemical Name:(1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate
CAS No.:1354948-03-0
Molecular Formula:C₁₂H₈F₃N₅O₃
Molecular Weight:327.222
Hs Code.:

Synonyms:(1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

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Chemical Property of (1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

Chemical Property:

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Technology Process of (1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

There total 4 articles about (1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354948-02-9
2-({4-cyano-3-[(trifluoromethyl)oxy]phenyl}amino)-2-oxoethyl acetate

: 1354948-03-0
(1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

Guidance literature:: 2-({4-cyano-3-[(trifluoromethyl)oxy]phenyl}amino)-2-oxoethyl acetate; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 0.5h;

With trimethylsilylazide; In tetrahydrofuran; at 20 ℃; for 4h; Reflux;

Reference yield:

: 609783-03-1
1,1-dimethylethyl {4-bromo-3-[(trifluoromethyl)oxy]phenyl}carbamate

: 1354948-03-0
(1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 15 h / Reflux

1.2: 2 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 4 h / 20 °C / Reflux

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 609783-06-4
4-amino-2-[(trifluoromethyl)oxy]benzonitrile

: 1354948-03-0
(1-{4-cyano-3-[(trifluoromethyl)oxy]phenyl}-1H-tetrazol-5-yl)methyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 4 h / 20 °C / Reflux

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;