C₄₈H₃₉BF₂IN₇

Base Information

• Chemical Name: C₄₈H₃₉BF₂IN₇
• CAS No.: 1228675-11-3
• Molecular Formula: C₄₈H₃₉BF₂IN₇
• Molecular Weight: 889.597
• Mol file: 1228675-11-3.mol

Synonyms:C₄₈H₃₉BF₂IN₇

Chemical Property of C₄₈H₃₉BF₂IN₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₈H₃₉BF₂IN₇

There total 3 articles about C₄₈H₃₉BF₂IN₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-(bis((6-(pyridin-2-yl)pyridin-2-yl)methyl)amino)benzaldehyde (1228675-10-2) + 4,4-difluoro-8-(4'-iodophenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene → C48H39BF2IN7 (1228675-11-3)

Guidance literature:

With piperidine; In toluene; for 12h; Reflux; Inert atmosphere;

DOI:10.1039/c0nj00770f

Reference yield:

6-bromomethyl-2,2'-bipyridine (83478-63-1) → C48H39BF2IN7 (1228675-11-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / acetonitrile / 120 h / 80 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; sodium formate / N,N-dimethyl-formamide / 3 h / 100 °C / 760.05 Torr / Inert atmosphere

3: piperidine / toluene / 12 h / Reflux; Inert atmosphere

With piperidine; bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; sodium formate; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; toluene; acetonitrile;

DOI:10.1039/c0nj00770f

Reference yield:

p-aminoiodobenzene (540-37-4) → C48H39BF2IN7 (1228675-11-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / acetonitrile / 120 h / 80 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; sodium formate / N,N-dimethyl-formamide / 3 h / 100 °C / 760.05 Torr / Inert atmosphere

3: piperidine / toluene / 12 h / Reflux; Inert atmosphere

With piperidine; bis-triphenylphosphine-palladium(II) chloride; carbon monoxide; sodium formate; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; toluene; acetonitrile;

DOI:10.1039/c0nj00770f

upstream raw materials:

4-(bis((6-(pyridin-2-yl)pyridin-2-yl)methyl)amino)benzaldehyde

6-bromomethyl-2,2'-bipyridine

p-aminoiodobenzene

Downstream raw materials:

C₇₈H₇₆BF₂N₇O₄Si

C₉₄H₈₅B₂F₄N₉O₄

C₅₀H₄₀BF₂N₇

C₅₃H₄₈BF₂N₇Si