[Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl₃]2

Base Information

• Chemical Name: [Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl₃]2
• CAS No.: 332941-53-4
• Molecular Formula: C₄₂H₄₂Cl₆Cr₂N₈P₂
• Molecular Weight: 1037.51

Synonyms:[Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl₃]2

Chemical Property of [Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl₃]2

Chemical Property:

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Technology Process of [Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl₃]2

There total 1 articles about [Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl₃]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

trichlorotris(tetrahydrofuran)chromium(III) (10170-68-0,16997-54-9) + 2-[(Diphenylphosphino)(1-methyl-1H-imidazol-2-yl)methyl]-1-methyl-1H-imidazole (332941-40-9) → [Cr((2-(diphenylphosphino)(N-methylimidazol-2-yl)methyl)-N-methylimidazole)Cl3]2 (332941-53-4)

Guidance literature:

In dichloromethane; a soln. of ligand in CH2Cl2 was added to a soln. of complex in CH2Cl2, the mixt. was stirred for 12 h (N2); the solvent was sepd., the product was stirred in CH2Cl2 overnight, CH2Cl2 was removed, ppt. was washed with CH2Cl2 and hexane, dried in vac.; elem. anal.;

DOI:10.1021/om000846b

upstream raw materials:

trichlorotris(tetrahydrofuran)chromium(III)

2-[(Diphenylphosphino)(1-methyl-1H-imidazol-2-yl)methyl]-1-methyl-1H-imidazole

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