3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

Base Information

Chemical Name:3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate
CAS No.:1236001-04-9
Molecular Formula:C₂₀H₂₄BrClN₂O₃
Molecular Weight:455.779
Hs Code.:

Synonyms:3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

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Chemical Property of 3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

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Technology Process of 3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

There total 1 articles about 3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1236001-03-8
3-(4-bromophenyl)-5-chloro-2,6-dimethyl-1-oxido-4-pyridinyl bis(1-methylethyl) carbamate

: 1236001-04-9
3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

: 1236001-05-0
3-(4-bromophenyl)-5-chloro-6-(hydroxymethyl)-2-methyl-4-pyridinyl bis(1-methylethyl)carbamate

Guidance literature:: 3-(4-bromophenyl)-5-chloro-2,6-dimethyl-1-oxido-4-pyridinyl bis(1-methylethyl) carbamate; With acetic anhydride; at 140 ℃; for 3h; Reflux;

With sodium hydroxide; In methanol; water; at 20 ℃; for 12h;

Reference yield:

: 1236001-04-9
3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

: 1236001-05-0
3-(4-bromophenyl)-5-chloro-6-(hydroxymethyl)-2-methyl-4-pyridinyl bis(1-methylethyl)carbamate

: 1236001-10-7
1-{[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]methyl}-4-{4-[(trifluoromethyl)oxy]phenyl} piperidine

: 76-05-1
trifluoroacetic acid

: 1236001-09-4
3-chloro-2-(hydroxymethyl)-6-methyl-5-{4'-[(4-{4-[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

: 1236001-07-2
3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

Guidance literature:: 3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate; 3-(4-bromophenyl)-5-chloro-6-(hydroxymethyl)-2-methyl-4-pyridinyl bis(1-methylethyl)carbamate; 1-{[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]methyl}-4-{4-[(trifluoromethyl)oxy]phenyl} piperidine; With barium(II) hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane; water; at 80 ℃; for 12h; Inert atmosphere;

trifluoroacetic acid; In water; acetonitrile;