3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

Base Information

Chemical Name:3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt
CAS No.:1236001-07-2
Molecular Formula:C₂HF₃O₂*C₃₉H₄₃ClF₃N₃O₄
Molecular Weight:824.26
Hs Code.:

3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

Synonyms:3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

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Chemical Property of 3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

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Technology Process of 3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

There total 1 articles about 3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1236001-04-9
3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate

: 1236001-05-0
3-(4-bromophenyl)-5-chloro-6-(hydroxymethyl)-2-methyl-4-pyridinyl bis(1-methylethyl)carbamate

: 1236001-10-7
1-{[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]methyl}-4-{4-[(trifluoromethyl)oxy]phenyl} piperidine

: 76-05-1
trifluoroacetic acid

: 1236001-09-4
3-chloro-2-(hydroxymethyl)-6-methyl-5-{4'-[(4-{4-[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

: 1236001-07-2
3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

Guidance literature:: 3-(4-bromophenyl)-5-chloro-2-(hydroxymethyl)-6-methyl-4-pyridinyl bis(1-methylethyl) carbamate; 3-(4-bromophenyl)-5-chloro-6-(hydroxymethyl)-2-methyl-4-pyridinyl bis(1-methylethyl)carbamate; 1-{[4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenyl]methyl}-4-{4-[(trifluoromethyl)oxy]phenyl} piperidine; With barium(II) hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane; water; at 80 ℃; for 12h; Inert atmosphere;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 1236001-07-2
3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt

: 1236000-43-3
3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4-[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4(1H)-pyridinone

Guidance literature:: 3-chloro-6-(hydroxymethyl)-2-methyl-5-{4'-[(4-{4[(trifluoromethyl)oxy]phenyl}-1-piperidinyl)methyl]-4-biphenylyl}-4-pyridinyl bis(1-methylethyl)carbamate trifluoroacetate salt; With hydrogenchloride; In methanol; water; for 3h; Reflux;

With sodium hydroxide; In water;