(2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

Base Information

Chemical Name:(2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid
CAS No.:139545-52-1
Molecular Formula:C₂₃H₂₉NO₂
Molecular Weight:351.489
Hs Code.:

Synonyms:(2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

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Chemical Property of (2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

Chemical Property:

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Technology Process of (2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

There total 3 articles about (2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 139545-46-3
2-(2,4,6-Trimethylphenyl)-3-oxo-3-phenylpropansaeure-piperidid

: 139545-52-1
(2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

Guidance literature:: With zinc(II) tetrahydroborate; zinc(II) chloride; In diethyl ether; at -15 ℃; for 5h;

Reference yield:

: 110-89-4
piperidine

: 139545-52-1
(2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / cyclohexane / Heating

2: 91 percent / Zn(BH₄)2/ZnCl₂ / diethyl ether / 5 h / -15 °C

With zinc(II) tetrahydroborate; zinc(II) chloride; In diethyl ether; cyclohexane;

Reference yield:

: 42797-62-6
2-Diazo-1-phenyl-3-(2,4,6-trimethylphenyl)-1,3-propandion

: 139545-52-1
(2R,3R)-und (2S,3S)-3-Hydroxy-2-(2,4,6-trimethylphenyl)-3-phenylpropansaeure-piperidid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / cyclohexane / Heating

2: 91 percent / Zn(BH₄)2/ZnCl₂ / diethyl ether / 5 h / -15 °C

With zinc(II) tetrahydroborate; zinc(II) chloride; In diethyl ether; cyclohexane;