tris[(benzyloxy)methyl]aminomethane

Base Information

Chemical Name:tris[(benzyloxy)methyl]aminomethane
CAS No.:401894-77-7
Molecular Formula:C₂₅H₂₉NO₃
Molecular Weight:391.51
Hs Code.:

Synonyms:tris[(benzyloxy)methyl]aminomethane

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Chemical Property of tris[(benzyloxy)methyl]aminomethane

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Technology Process of tris[(benzyloxy)methyl]aminomethane

There total 1 articles about tris[(benzyloxy)methyl]aminomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 401894-77-7
tris[(benzyloxy)methyl]aminomethane

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / KOH / dimethylformamide / 2 h / 20 °C

2: 97 percent / TFA / CH₂Cl₂ / 4 h / 20 °C

With potassium hydroxide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2001-18065

Reference yield: 90.3%

: 13726-67-5
Boc-Asp-OH

: 401894-77-7
tris[(benzyloxy)methyl]aminomethane

: [1,2-bis-(2-benzyloxy-1,1-bis-benzyloxymethyl-ethylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl acetamide; at 20 ℃; for 15h;
DOI:10.1021/ja045263y