2,2-difluoroethenylxenon(II) tetrafluoroborate

Base Information

• Chemical Name: 2,2-difluoroethenylxenon(II) tetrafluoroborate
• CAS No.: 726203-13-0
• Molecular Formula: BF₄*C₂HF₂Xe
• Molecular Weight: 281.121
• Mol file: 726203-13-0.mol

Synonyms:2,2-difluoroethenylxenon(II) tetrafluoroborate

Chemical Property of 2,2-difluoroethenylxenon(II) tetrafluoroborate

Chemical Property:

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Technology Process of 2,2-difluoroethenylxenon(II) tetrafluoroborate

There total 1 articles about 2,2-difluoroethenylxenon(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

xenon difluoride (13709-36-9) + (2,2-difluorovinyl)difluoroborane (37842-97-0) → 1,1,1,2,2-pentafluoroethane (354-33-6) + 2,2-difluoroethenylxenon(II) tetrafluoroborate (726203-13-0)

Guidance literature:

In further solvent(s); soln. of CF2=CHBF2 in 1,1,1,3,3-pentafluoropropane and 1,1,1,3,3-pentafluorobutane cooled to -60°C and XeF2 added in one portion; stirredat -60 to -62°C for 2 h and left for 15 min without stirring; decanted; precipitate treated in vacuum at -60°C; unknown byproducts detected by NMR;

DOI:10.1002/zaac.200300224

upstream raw materials:

xenon difluoride

(2,2-difluorovinyl)difluoroborane

Refernces