N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

Base Information

Chemical Name:N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide
CAS No.:917513-91-8
Molecular Formula:C₁₈H₁₁BrF₁₀N₂OS
Molecular Weight:573.252
Hs Code.:

Synonyms:N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

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Chemical Property of N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

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Technology Process of N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

There total 5 articles about N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 917513-83-8
N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-aminobenzamide

: 917513-91-8
N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

Guidance literature:: N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-aminobenzamide; With sulfuric acid; at 0 - 5 ℃; for 0.166667h;

formaldehyd; In water; at 0 - 5 ℃; for 3h;

Reference yield:

: 347-55-7
2-aminophenyl trifluoromethyl sulfide

: 917513-91-8
N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium dithionite; sodium hydrogencarbonate / tetra(n-butyl)ammonium hydrogensulfate / tert-butyl methyl ether; water / 10 h / 20 °C

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 20 °C

3.1: pyridine / 10 h / 90 °C

3.2: 0 °C / pH 1

3.3: 21.5 h / 0 - 20 °C

4.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 3 h / 60 °C

4.2: 0 - 60 °C

5.1: sulfuric acid / 0.17 h / 0 - 5 °C

5.2: 3 h / 0 - 5 °C

With pyridine; hydrogenchloride; N-Bromosuccinimide; sodium dithionite; sulfuric acid; sodium hydrogencarbonate; tin(ll) chloride; tetra(n-butyl)ammonium hydrogensulfate; In ethanol; tert-butyl methyl ether; water; N,N-dimethyl-formamide;

Reference yield:

: 917513-74-7
2-bromo-4-heptafluoroisopropyl-6-(trifluoromethylthio)aniline

: 917513-91-8
N-(2-bromo-4-heptafluoroisopropyl-6-trifluoromethylthio)phenyl 3-(methylamino)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 10 h / 90 °C

1.2: 0 °C / pH 1

1.3: 21.5 h / 0 - 20 °C

2.1: hydrogenchloride; tin(ll) chloride / ethanol; water / 3 h / 60 °C

2.2: 0 - 60 °C

3.1: sulfuric acid / 0.17 h / 0 - 5 °C

3.2: 3 h / 0 - 5 °C

With pyridine; hydrogenchloride; sulfuric acid; tin(ll) chloride; In ethanol; water;