C₄₈H₅₇N₉O₆

Base Information

Chemical Name:C₄₈H₅₇N₉O₆
CAS No.:1613056-45-3
Molecular Formula:C₄₈H₅₇N₉O₆
Molecular Weight:856.037
Hs Code.:

C<sub>48</sub>H<sub>57</sub>N<sub>9</sub>O<sub>6</sub>

Synonyms:C₄₈H₅₇N₉O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₈H₅₇N₉O₆

Chemical Property:

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Technology Process of C₄₈H₅₇N₉O₆

There total 21 articles about C₄₈H₅₇N₉O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1228552-50-8
(((S)-3-methyl-1-oxo-1-((S)-2-(6-(4,4,5,5-tetramethyl-1,3,2-dioxolo)ethylpentocycloboran-2-yl)-1H-benzo[d]imidazol-2-yl)pyrrolidin-1-yl)propan-2-yl)carbamate

: 1613056-44-2
C₃₁H₃₄F₃N₅O₆S

: 1613056-45-3
C₄₈H₅₇N₉O₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 4h; Inert atmosphere; Sealed tube;

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1613056-45-3
C₄₈H₅₇N₉O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Sealed tube

1.2: 4 h / 0 - 20 °C / Inert atmosphere; Sealed tube

2.1: acetic acid / 40 °C / Inert atmosphere; Sealed tube

3.1: hydrogenchloride / ethyl acetate / 8 h / 0 - 20 °C / Inert atmosphere; Sealed tube

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere; Sealed tube

6.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: (S)-5-(4-bromophenyl)-2-(pyrrolidin-2-yl)-1H-imidazole dihydrochloride

: 1613056-45-3
C₄₈H₅₇N₉O₆

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere; Sealed tube

3: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

4: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 4 h / 90 °C / Inert atmosphere; Sealed tube

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;