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C30H37N3O5

Base Information
  • Chemical Name:C30H37N3O5
  • CAS No.:1613625-30-1
  • Molecular Formula:C30H37N3O5
  • Molecular Weight:519.641
  • Hs Code.:
C<sub>30</sub>H<sub>37</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C30H37N3O5

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Chemical Property of C30H37N3O5
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Technology Process of C30H37N3O5

There total 17 articles about C30H37N3O5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C22H31N3O3*C2H4O2; With sodium hydrogencarbonate; In methanol; water; at 0 ℃; for 0.166667h;
benzyl chloroformate; In methanol; water; at 0 - 20 ℃; for 2h;
Guidance literature:
Multi-step reaction with 17 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C
1.2: 36 h / 20 °C
2.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr
3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C
4.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C
4.2: 1.8 h / -78 - 20 °C
5.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C
5.2: 0.08 h / -78 °C
5.3: 16 h / -78 - 24 °C
6.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.2 h / 0 - 20 °C
7.1: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr
8.1: acetic acid; hydrogen bromide / 3 h / Reflux
9.1: acetyl chloride / 4 h / 0 °C / Reflux
10.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C
11.1: pyridine / 2 h / 0 - 20 °C
12.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux
13.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C
14.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 2 h / 0 °C
15.1: ammonia / methanol / 18 h / 0 - 20 °C
16.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr
17.1: sodium hydrogencarbonate / methanol; water / 0.17 h / 0 °C
17.2: 2 h / 0 - 20 °C
With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; cyclohexane; water; acetonitrile;
Guidance literature:
Multi-step reaction with 14 steps
1.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C
1.2: 1.8 h / -78 - 20 °C
2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C
2.2: 0.08 h / -78 °C
2.3: 16 h / -78 - 24 °C
3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.2 h / 0 - 20 °C
4.1: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr
5.1: acetic acid; hydrogen bromide / 3 h / Reflux
6.1: acetyl chloride / 4 h / 0 °C / Reflux
7.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C
8.1: pyridine / 2 h / 0 - 20 °C
9.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux
10.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C
11.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 2 h / 0 °C
12.1: ammonia / methanol / 18 h / 0 - 20 °C
13.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr
14.1: sodium hydrogencarbonate / methanol; water / 0.17 h / 0 °C
14.2: 2 h / 0 - 20 °C
With 4-methyl-morpholine; pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; cyclohexane; water; acetonitrile;
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